tailieunhanh - Synthesis of silica nanoparticles from rice husk ash
The X-ray diffraction (XRD) pattern with only one peak at 2θ ~ 220 confirmed the amorphous phase of SiO2 NPs. The Fourier transform infrared (FTIR) and energydispersive X-ray (EDX) spectra were also used to evaluate the functional groups and the purity of SiO2 NPs. The SiO2 NPs powder with high purity could be suitably produced by calcination of acid treated RHA at 7000 C for 2h. | 50 SCIENCE & TECHNOLOGY DEVELOPMENT JOURNAL, Vol 20, 2017 Synthesis of silica nanoparticles from rice husk ash Dang Thi Thuy Nhung, Tran Hoa, Nguyen Thuy Ai Trinh, Dang Van Phu, Phan Dinh Tuan, Nguyen Quoc Hien Abstract— Silica nanoparticles (SiO2 NPs) were synthesized from rice husk ash (RHA) by chemical treatment and calcination. The size of SiO2 NPs evaluated by transmission electron microscope (TEM) was of 20 - 50 nm and the size distribution of SiO2 NPs measured by dynamic laser scattering (DLS) was of Gaussian mode. The X-ray diffraction (XRD) pattern with only one peak at 2θ ~ 220 confirmed the amorphous phase of SiO2 NPs. The Fourier transform infrared (FTIR) and energydispersive X-ray (EDX) spectra were also used to evaluate the functional groups and the purity of SiO2 NPs. The SiO2 NPs powder with high purity could be suitably produced by calcination of acid treated RHA at 7000C for 2h. The obtained SiO2 NPs product can be potentially used for numerous purposes of application, especially as filler in paints. Index Terms— silica nano, rice husk ash, calcination, particle size. 1 INTRODUCTION Rice husk (RH) is a byproduct of rice milling process and RH is one of the abundant waste sources in rice growing countries such as Vietnam, Thailand, China,. It is estimated that one ton of Manuscript Received on June 12th, 2017, Manuscript Revised November 18th, 2017. Dang Thi Thuy Nhung, Nguyen Thuy Ai Trinh, Phan Dinh Tuan - Ho Chi Minh City of Natural Resources and Environment, 263B Le Van Sy Street, Ho Chi Minh City, Vietnam Tran Hoa - University of Science, Vietnam National University in Ho Chi Minh City, 227 Nguyen Van Cu Street, Ho Chi Minh City, Vietnam. Dang Van Phu, Nguyen Quoc Hien - Research and Development Center for Radiation Technology, Vietnam Atomic Energy Institute, 202A Street 11, Linh Xuan Ward, Thu Duc District, Ho Chi Minh City, Vietnam * Corresponding author. Email: dthnhung@ rice is created ~ ton of RH. .
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